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 首頁 > 產品展示 > 安捷倫液相色譜儀 > 液相色譜儀 > 安捷倫1260熒光檢測器G1321B
 
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產品型號:
安捷倫1260熒光檢測器
產品名稱:
安捷倫1260熒光檢測器G1321B
產品報價:
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  安捷倫1260熒光檢測器安捷倫1260熒光檢測器G1321B的詳細資料:
  

安捷倫1260熒光檢測器(G1321B

 

 

介紹

 

The detector is designed for highest optical performance, GLP compliance and

easy maintenance. It includes the following features:

flash lamp for highest intensity and lowest detection limit

multi-wavelength mode for on-line spectra

spectra acquisition and simultaneous multi-signal detection

optional cuvette is available and can be used for off-line measurements

easy front access to flow cell for fast replacement and

built-in wavelength accuracy verification.

 

 

參數

 

Type

Specification

Comments

Detection type

Multi-signal fluorescence detector withrapid on-line scanning capabilities and

spectral data analysis

 

Performance specifications

Single wavelength operation:

RAMAN (H2O) > 500 (noise reference

measured at signal)

Ex=350 nm, Em=397 nm, dark value

450 nm, standard flow cell

RAMAN (H2O) > 3000 (noise reference

measured at dark value)

Ex=350 nm, Em=397 nm, dark value

450 nm, standard flow cell

Dual wavelength operation:

RAMAN (H2O) > 300 Ex 350 nm, Em

397 nm and Ex 350 nm, Em 450 nm,

standard flow cell.

Light source

Xenon Flash Lamp, normal mode 20 W,

economy mode 5 W, lifetime 4000 h

 

Pulse frequency

296 Hz for single signal mode

74 Hz for economy mode

 

Maximum data rate

74 Hz

 

Excitation monochromator

Range: settable 200 nm - 1200 nm and

zero-order

Bandwidth: 20 nm (fixed)

Monochromator: concave holographic

grating, F/1.6, blaze: 300 nm

 

Emission monochromator

Range: settable 200 nm - 1200 nm and

zero-order

Bandwidth: 20 nm (fixed)

Monochromator: concave holographic

grating, F/1.6, blaze: 400 nm

 

Reference system

in-line excitation measurement

 

Timetable programing

up to 4 signal wavelengths, response time,

PMT Gain, baseline behavior (append,

free, zero), spectral parameters

 

Spectrum acquisition

Excitation or Emission spectra

Scan speed: 28 ms per datapoint (e.g.

0.6 s/spectrum 200 400 nm, 10 nm step)

Step size: 1 20 nm

Spectra storage: All

 

Wavelength characteristic

Repeatability +/- 0.2 nm

Accuracy +/- 3 nm setting

 

Flow cells

Standard: 8 ul volume and 20 bar (2MPa) pressure maximum, quartz

Optional:

Fluorescence cuvette for offline

spectroscopic measurements with

1 mL syringe, 8 ul volume, quartz

Bio-inert: 8 ul volume and 20 bar

(2 MPa) pressure maximum, sapphire

(pH 112)

Micro: 4 ul volume and 20 bar (2 MPa)

pressure maximum, quartz

 

Control and data evaluation

Agilent ChemStation for LC, Agilent

Instant Pilot G4208A with limited spectral

data analysis and printing of spectra

 

Analog outputs

Recorder/integrator: 100 mV or 1 V,

output range > 100 LU, two outputs

100 LU is the

recommended range,

see "FLD Scaling

Range and Operating

Conditions"

Communications

Controller-area network (CAN), RS-232C,

LAN, APG

Remote: ready, start, stop and shut-down

signals

 

Safety and maintenance

Extensive diagnostics, error detection and

display (through Instant Pilot G4208A and

ChemStation), leak detection, safe leak

handling, leak output signal for shutdown

of pumping system. Low voltages in major

maintenance areas.

 

GLP features

Early maintenance feedback (EMF) for

continuous tracking of instrument usage

in terms of lamp burn time with

user-settable limits and feedback

messages. Electronic records of

maintenance and errors. Verification of

wavelength accuracy, using the Raman

band of water.

 

Housing

All materials recyclable

 

Environment

0 40 °C constant temperature at <95 %

humidity (non-condensing)

 

Dimensions

140 mm x 345 mm x 435 mm

(5.5 x 13.5 x 17 inches)

(height x width x depth

 

Weight

11.5 kg (25.5 lbs)

 

 

 

 

配件與耗材

 

Overview of Maintenance Parts

 

 

p/n

Description

G1321-60005

Flow cell, 8 μL, 20 bar (pH 19.5)

G1321-60015

Flow cell, 4 μL, 20 bar (pH 19.5) requires a 0.12 mm i.d. capillary (e.g. p/n

G1316-87318, 300 mm long), part of Capillary kit for 0.12 mm id (p/n

G1316-68716)

G5615-60005

Bio-inert flow cell, 8 μL, 20 bar (pH 112) includes Capillary Kit Flow Cells BIO

(p/n G5615-68755))

G5615-68755

Capillary Kit Flow Cells BIO includes Peek Capillary i.d. 0.18 mm, 1.5 m lg and

PEEK Fittings 10/PK (p/n 5063-6591)

G1321-60007

FLD Cuvette Kit, 8 μL, 20 bar

9301-0407

Needle

9301-1446

Syringe

5067-4691

Front Panel DAD/VWD/FLD (1260/1290)

5041-8388

Leak funnel

5041-8389

Leak funnel

5041-8387

Tube clip

5062-2463

Corrugated tubing, PP, 6.5 mm id, 5 m

5062-2462

PTFE Tubing flexible i.d. 0.8 mm, o.d. 1.6 mm, 2 m, re-order 5 m (flow cell to waste)

5181-1516

CAN cable, Agilent module to module, 0.5 m

5181-1519

CAN cable, Agilent module to module, 1 m

G1369B or G1369-60002

Interface board (LAN)

5023-0203

Cross-over network cable, shielded, 3 m (for point to point connection)

5023-0202

Twisted pair network cable, shielded, 7 m (for point to point connection)

01046-60105

Agilent module to general purpose (Analog)

G1351-68701

Interface board (BCD) with external contacts and BCD outputs

 

 

Cuvette Kit

 

p/n

Description

G1321-60007

FLD Cuvette Kit, 8 μL, 20 bar includes

5062-2462

PTFE Tubing flexible i.d. 0.8 mm, o.d. 1.6 mm, 2 m, re-order 5 m (flow cell to waste)

PTFE Tubing flexible i.d. 0.8 mm, o.d. 1.6 mm, 2 m, re-order 5 m (flow cell to waste)

SST Fitting

0100-0043

SST front ferrule

0100-0044

SST back ferrule

0100-1516

Fitting male PEEK, 2/pk

9301-0407

Needle

9301-1446

Syringe

 

 

Standard Accessory Kit

 

Accessory kit (p/n G1321-68755) contains some accessories and tools needed

for the installation and repair/calibration of the detector.

 



 

 

Item

p/n

Description

1

5062-2462

PTFE Tubing flexible i.d. 0.8 mm, o.d. 1.6 mm, 2 m, re-order 5 m (flow cell to waste)

2

0100-1516

Fitting male PEEK, 2/pk

3

G1315-87311

Capillary column detector 380 mm lg, 0.17 i.d., (includes SST ferrule front, SST ferrule back and SST fitting).

4

0100-0043

SST front ferrule

5

0100-0044

SST back ferrule

6

79814-22406

SST Fitting

 

Capillary Kit Flow Cells BIO

 

Capillary Kit Flow Cells BIO includes Peek Capillary i.d. 0.18 mm, 1.5 m lg and

PEEK Fittings 10/PK (p/n 5063-6591) (p/n G5615-68755) includes

p/n

Description

0890-1763

Peek Capillary i.d. 0.18 mm, 1.5 m lg

5063-6591

PEEK Fittings 10/PK

 

Overview of Main Assemblies

 

Item

p/n

Description

1

G1321-65000

Detector main board (FLM) - NEW (G1321B)

1

G1321-69000

EXCH Detector main board (FLM) (G1321B

1

G1321-66500

Detector main board (FLM) - NEW (G1321A)

1

G1321-69500

EXCH Detector main board (FLM) (G1321A)

 

1251-7788

Hexagonal Nut for APG and COM port (4x)

 

2940-0256

Nut M14 analog output

 

2190-0699

Washer analog output

 

5181-1516

CAN cable, Agilent module to module, 0.5 m

2

0950-2528

Power supply

3

G1351-68701

Interface board (BCD) with external contacts and BCD outputs

3

G1369B or

G1369-60002

LAN Communication Interface board,

3

G1369C or

G1369-60012

LAN Communication Interface board

2110-0004

Fuse for BCD board, 250 mA

4

3160-1017

Fan assembly

5

G1321-69002

Optical unit (exchange assembly)

6

2140-0600

Flash lamp

7

1000-1000

Mirror assembly

8

G1321-60003

EX Grating assembly (includes protection ring)

9

G1321-60004

EM Grating assembly (includes protection ring)

10

1970-0201

Photo-multiplier Tube (PMT),

11

1000-1124

Condenser assembly EM

12

G1321-60005

Standard flow cell, 8 μL, 20 bar

13

5061-3356

Leak sensor

14

G1321-61600

Cable FLM - FLF board

 

 

 

Optical Unit Assembly

 

Item

p/n

Description

 

G1321-60002

Optical unit - NEW (comes with foam part and cable FLM/FLF)

 

G1321-69002

Optical unit (exchange assembly)

1

G1321-66512

FLL Board (includes trigger pack)

2

2140-0600

Flash lamp

3

1000-1136

EX condenser Assembly

4

G1321-08103

Slit EX

5

1000-1000

Mirror assembly

6

G1321-60003

EX Grating assembly (includes protection ring)

7

G1321-60004

EM Grating assembly (includes protection ring)

8

G1321-60005

Flow cell, 8 μL, 20 bar (pH 19.5)

G1321-60015

Flow cell, 4 μL, 20 bar (pH 19.5)

G5615-60005

Bio-inert flow cell, 8 μL, 20 bar (pH 112) includes Capillary Kit Flow Cells BIO (p/n G5615-68755))

G5615-68755

Capillary Kit Flow Cells BIO includes Peek Capillary i.d. 0.18 mm, 1.5 m lg and PEEK Fittings 10/PK (p/n 5063-6591)

G1321-60007

FLD Cuvette Kit, 8 μL, 20 bar

G1321-22400

Screw for flow cell / cuvette

9

G1321-08102

Slit EM (also used for PMT)

10

1970-0201

Photo-multiplier Tube (PMT),

11

1000-1124

Condenser assembly EM

12

G1321-66531

Front-end Board (FLF) Rev D, underneath the optical (new) (requires firmware revision A.04.06 or above)

12

G1321-69531

FLF Board (requires firmware revision A.04.06 or above), FLR Reference Diode board G1321-66533

13

G1321-66533

FLR Reference Diode board

14

1000-1121

Diffuser plate (in front of the reference diode board FLR)

15

5062-8530

Cutoff filter 295 nm

16

01046-42701

Carbon filter mat

17

G1321-61600

Cable FLM - FLF board

G1321-40103

Foam Optics

18

G1321-61602

Cable chassis

19

0515-2574

Screw M5 x 25 mm, for chassis cable

 

0515-1052

Screw 2.5 mm hex for monochromator, lamp pad, condenser #1, slits, etc

 

0515-2548

Screw M4 x 25 mm hex, for lamp housing

 

0515-2549

Screw M4 x 8 mm, for FLF board

 

Photo-muliplier Tubes and Cutoff Filters

 

 

p/n

Description

5061-3327

Cutoff filter kit: 389 nm, 408 nm, 450 nm, 500 nm, 550 nm

5061-3328

Cutoff filter kit: 380 nm, 399 nm, 418 nm, 470 nm, 520 nm

5061-3329

Cutoff filter kit: 280 nm, 295 nm, 305 nm, 335 nm, 345 nm

1000-0822

Cutoff filter 370 nm

R928HA

Photo-multiplier Tube (PMT, 185 to 900 nm); contact Hamamatsu dealers

R3788HA

Photo-multiplier Tube (PMT, 185 to 750 nm); contact Hamamatsu dealers

 

Lamp Cover Parts

 

Item

p/n

Description

1

G1321-08100

Plate

2

0515-1052

Screw 2.5 mm hex for monochromator, lamp pad, condenser #1, slits, etc.

3

1000-0999

Quartz Window

 

Sheet Metal Kit








Item 

p/n

Description

 

G1321-68701

Sheet metal kit includes case and top cover

 

5022-2112

Screw cover

 

Plastic Parts







Item

p/n

Description

1

5067-4691

Front Panel DAD/VWD/FLD (1260/1290)

2

5065-9985

 Cover kit (includes base, top, left and right)

3

5043-0207

Name plate 1260

 

Foam Parts









Item

p/n

Description

1.2

G1321-68702

EPP foam kit, includes bottom and top rear

3

G1321-68700

Foam Pads (located underneath the optical), set of two

4

5041-8395

Foam kit (includes top and bottom foam).

 

Power and Status Light Pipes








 

Item

p/n

Description

 

0950-2528

Power supply

 

0515-0910

Screw M4 x 0.7, 8 mm lg, to fix power supply at rear panel

 

2190-0409

Washer

1

5041-8382

Power switch light pipe

2

5041-8384

Status light pipe

3

5041-8381

Power switch button

4

5041-8383

Power switch coupler

 

Leak Parts








 

Item

p/n

Description

1

5061-3356

Leak sensor

2

G1321-40511

Leak Pan

3

5041-8388

Leak funnel

4

5041-8389

Leak funnel holder

5.6

5042-9974

Tubing Flex (1.5 m)

5.6

5062-2463

Corrugated tubing, PP, 6.5 mm id, 5 m



 

 

 

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